Determination of residual formamide in allopurinol by gas chromatography

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- Determination of residual formamide in allopurinol by gas chromatography
- Journal of Chongqing Medical University Issue 11, Pages: 1208-1209(2007)
- 作者机构：
  
  1. 重庆医科大学附属儿童医院药剂科
  2. 重庆市中药研究院
- 作者简介：
- 基金信息：
- DOI：
  CLC： R927
- Published：2007，
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[1]罗佳,喻强.气相色谱法测定别嘌醇中甲酰胺残留[J].重庆医科大学学报,2007(11):1208-1209+1220.

LUO Jia, et al. Determination of residual formamide in allopurinol by gas chromatography. [J]. Journal of Chongqing Medical University (11):1208-1209(2007)
[1]罗佳,喻强.气相色谱法测定别嘌醇中甲酰胺残留[J].重庆医科大学学报,2007(11):1208-1209+1220. DOI：

LUO Jia, et al. Determination of residual formamide in allopurinol by gas chromatography. [J]. Journal of Chongqing Medical University (11):1208-1209(2007) DOI：

目的:建立别嘌醇中甲酰胺残留量气相色谱测定方法。方法:采用氢火焰离子化检测器（FID）

SUPLCOWAX-10柱分离。结果:甲酰胺在5～20μg/ml的浓度范围内呈良好的线性关系

平均回收率为95.57%（RSD=1.74%

n=6）。结论:本法适用于别嘌醇中甲酰胺残留量的测定。

Objective:To establish method for determination of residual formamide in Allopurinol by gas chromato-graphy.Methods:Detected by FID detector

Separated by SUPLCOWAX-10.Results:The formamide show a good linear relationship at range of 5～20μg/ml

the average recovery was 95.57%.(RSD=1.74%

n=6)for formamide.Conclusion:It is quite suitable to be used in analysis of the formamide in Allopurinol.

别嘌醇甲酰胺残留气相色谱

AllopurinolResidual formamideGas chromatography

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